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Advanced analysis of (emerging) organic trace contaminants in the harbours of Oostende and Zeebrugge and the Belgian coastal zone: steroidal EDC's, plasticizers and plastic additives
Citation
Huysman, S.; Vanhaecke, L.; Laboratory for Chemical Analysis (LCA). Ugent: Belgium; (2020): Advanced analysis of (emerging) organic trace contaminants in the harbours of Oostende and Zeebrugge and the Belgian coastal zone: steroidal EDC's, plasticizers and plastic additives. https://marineinfo.org/id/dataset/6343

Availability: Unrestricted after moratorium period
Data are initially restricted, but the access condition relaxes to academic or unrestricted once a specified period of time after an event (such as collection, publication, completion of QC procedures or project cessation) has elapsed

Description
Dataset on polar micropollutants (endocrine disrupting compounds and phthalates). more

Within the current legislative context regarding the monitoring of our aqueous bodies, a number of priority compounds are included in the European Water and Marine Strategy Framework Directives and in the Coordinated Environmental Monitoring Programme (CEMP) of the OSPAR commission. However, several other so-called emerging micropollutants are not regulated yet. So, new monitoring approaches need to include these emerging contaminants. Therefore, within NewSTHEPS, the research group LCA focuses on both the method development and application of quantitative monitoring of marine waters towards the presence of targeted emerging polar micropollutants, including endocrine disrupting compounds and phthalates. Next, a qualitative screening of untargeted, non a-priori selected, (known and/or unknown) micropollutants and metabolites is foreseen. To this extent, advanced multi-residue methods using liquid-chromatography (LC) and high-resolution mass spectrometry (HRMS; Q-Exactive™, Thermo Fisher Scientific) will be developed and validated according to CD/2002/657/EC. The LC-part enables separation of a broad range of contaminants with different polarities and physical-chemical properties, whereas accurate mass measurements in full-scan HRMS facilitate rapid, robust and selective analysis for both quantitative and qualitative applications on the same samples.

Scope
Themes:
Biology > Organic (& bio-) chemistry, Coastal studies (e.g. shores, estuaries), Environmental quality/pollution
Keywords:
Marine/Coastal, Androgens, Corticosteroids, Divinylbenzene (DVB) Speedisk passive samplers, Oestrogens, Plasticizers, plastics additives, Progestins, Sex hormones, UHPLC-HRMS, ANE, Belgium, Belgian Coast, ANE, Belgium, Brugge, Zeebrugge Harbour, ANE, Belgium, Oostende Harbour

Geographical coverage
ANE, Belgium, Belgian Coast [Marine Regions]
ANE, Belgium, Brugge, Zeebrugge Harbour [Marine Regions]
ANE, Belgium, Oostende Harbour [Marine Regions]

Temporal coverage
2014 - 2019

Parameter
Concentration

Contributors
Vlaams Instituut voor de Zee (VLIZ), moredata manager
Koninklijk Belgisch Instituut voor Natuurwetenschappen; Departement Beheer van het Mariene Ecosysteem; Beheerseenheid Mathematisch Model Noordzee en Schelde-estuarium; Belgisch Marien Data Centrum (BMDC), moredata owner
Universiteit Gent; Faculteit Diergeneeskunde; Vakgroep Veterinaire Volksgezondheid & Voedselveiligheid; Laboratorium voor Chemische Analyse (LCA), moredata creatordata creator

Related datasets
Parent dataset:
NewSTHEPS project data for the harbours of Oostende and Zeebrugge and the Belgian coastal zone, more
Other relations:
Advanced analysis of (emerging) organic trace contaminants in the harbours of Oostende and Zeebrugge and the Belgian coastal zone: pesticides, pharmaceuticals and personal care products, more
Analysis of metals in the harbours of Oostende and Zeebrugge and the Belgian coastal zone, more
Ecotoxicity testing of environmentally realistic contaminant mixtures using passive samplers, more
Particulate carbon, nitrogen and stable isotope determination of Suspended Particulate Matter (SPM) in the harbours of Oostende and Zeebrugge and the Belgian coastal zone, more
Supporting water quality data for the NewSTHEPS sampling campaigns, more

Project
NewSTHEPS: New Strategies for monitoring and risk assessment of Hazardous chemicals in the marine Environment with Passive Samplers, more

Publication
Based on this dataset
Huysman, S. et al. (2019). Targeted quantification and untargeted screening of alkylphenols, bisphenol A and phthalates in aquatic matrices using ultra-high-performance liquid chromatography coupled to hybrid Q-Orbitrap mass spectrometry. Anal. Chim. Acta 1049: 141-151. https://dx.doi.org/10.1016/j.aca.2018.10.045, more
Huysman, S. et al. (2018). Have plasticizers already reached our marine environment?, in: Mees, J. et al. (Ed.) Book of abstracts – VLIZ Marine Science Day. Bredene, Belgium, 21 March 2018. VLIZ Special Publication, 80: pp. 15, more
Huysman, S. et al. (2018). UHPLC-HRMS based targeted and untargeted screening of plasticizers in the marine environment, in: 23rd National Symposium for Applied Biological Sciences (NSABS), Brussels (Belgium). Communications in Agricultural and Applied Biological Sciences, 83(1): pp. 1, more
Huysman, S. et al. (2018). A metabolomics approach towards identification of unknown emerging pollutants in marine waters, in: Benelux Metabolomics Days, 19-20 September Rotterdam, The Netherlands. , more
Huysman, S. et al. (2018). Divinylbenzene samplers as surrogate tool for biological monitoring of (micro)pollutants in the marine environment, in: ASSET 2018 summit on on Global Food Inegrity, 28-31 May 2018, Belfast, Ireland: Abstracts. , more
Vanryckeghem, F. et al. (2018). Screening of the Belgian Part of the North Sea towards emerging organic micropollutants: comparison of two SPE-techniques prior to UHPLC-Orbitrap-HRMS analysis, in: 23rd National Symposium for Applied Biological Sciences (NSABS), Brussels (Belgium). Communications in Agricultural and Applied Biological Sciences, 83(1): pp. 1-5, more
Vanryckeghem, F. et al. (2018). Ultra-trace analysis of pharmaceuticals and hormones in marine waters by using UHPLC-ORBITRAP-HRMS, in: Hormone and Veterinary Drug Residue Analysis: 8th International Symposium, Gent 22-25 May 2018: Abstract Book. pp. 39, more
Vanryckeghem, F. et al. (2018). Targeted screening by Orbitrap HRMS reveals the occurrence of pharmaceuticals, personal care products and pesticides in the Belgian Part of the North Sea, in: Mees, J. et al. (Ed.) Book of abstracts – VLIZ Marine Science Day. Bredene, Belgium, 21 March 2018. VLIZ Special Publication, 81: pp. 121, more
Huysman, S. et al. (2017). Development and validation of an ultra-high performance liquid chromatographic high resolution Q-Orbitrap mass spectrometric method for the simultaneous determination of steroidal endocrine disrupting compounds in aquatic matrices. Anal. Chim. Acta 984: 140-150. https://dx.doi.org/10.1016/j.aca.2017.07.001, more
Huysman, S. et al. (2017). Environmental forensics in seawater coupling a divinylbenzene passive sampling device and high resolution mass spectrometry for the screening of micropollutants, in: SETAC Europe 27th Annual meeting (SETAC Europe 2017): Environmental quality through transdisciplinary collaboration. Abstracts. , more
Huysman, S. et al. (2017). Environmental screening of organic micropollutants in seawater by coupling a divinylbenzene passive sampling device and high resolution mass spectrometry. Department of Veterinary Public Health and Food Safety, Ghent University: Ghent. , more
Huysman, S. et al. (2017). How far have plasticizers and additives penetrated our aquatic environment?, in: SETAC Europe 27th Annual meeting (SETAC Europe 2017): Environmental quality through transdisciplinary collaboration. Abstracts. , more
Huysman, S. et al. (2017). Targeted, suspected and non-target screening with high resolution mass spectrometry in the marine environment : ready to go? Poster presented at Belgian Metabolomics Day 2017. Department of Veterinary Public Health and Food Safety/Department of Sustainable Organic Chemistry and Technology: Gent. 1poster pp., more
Vanhaecke, L.; Huysman, S.; Van Meulebroek, L. (2017). Emerging contaminants and toxins in aquaculture : how modern analytical tools may aid to ensure food and environmental safety, in: SETAC Europe 27th Annual meeting (SETAC Europe 2017): Environmental quality through transdisciplinary collaboration. Abstracts. , more
Vanhaecke, L. et al. (2017). The central role of modern analytical tools in studying the link between oceans & human health. Universiteit Gent: Gent. , more
Vanryckeghem, F. et al. (2017). Measuring emerging organic micropollutants in the North Sea using high-resolution Orbitrap mass spectrometry : method validation and occurrence in harbour and open sea, in: SETAC Europe 27th Annual meeting (SETAC Europe 2017): Environmental quality through transdisciplinary collaboration. Abstracts. , more
Huysman, S. et al. (2016). Is the divinylbenzene passive sampler a useful tool for measuring hydrophilic endocrine disrupting compounds in the marine environment?, in: Passive Sampling, 8th International Workshop and Symposium, Prague, 7-10 September 2016. Abstracts. , more
Huysman, S. et al. (2016). Is our North Sea contaminated with endocrine disrupting compounds?, in: Degraer, S. et al. (Ed.) North Sea Open Science Conference 7-10/11/2016. Abstract Booklet. pp. 73, more
Huysman, S. et al. (2016). Passive samplers, as surrogates for biological monitoring, to measure emerging (micro)pollutants in the marine environment, in: Proceedings of EuroResidue VIII. Conference on Residues of Veterinary Drugs in Food 23-25 May 2016, Egmond aan Zee. pp. 481-485, more

Dataset status: In Progress
Data type: Data
Data origin: Research: field survey
Metadatarecord created: 2019-10-11
Information last updated: 2019-10-11
All data in the Integrated Marine Information System (IMIS) is subject to the VLIZ privacy policy